Need help with making test-e

[jeebise23]

hey guys this post has been revised, i am having problems with my whatman 45u getting clogged after my 2nd 10ml try. this is how i started and finished.first i put 50 grams of test-e powder in a beeker then i put 2%=4ml of ba in, then 18%=36 ml of bb. I added this to the powder to disolve it. I also had the beeker inside a pan with water in it and the temp. on low, and stirred it until everything was dissolve. Once that was complete i put cottonseed oil to the mixture i left the sove on low and kept stirring until i felt that it was enough. Now alot of you guys say that it should already look clear and yellow, well mine was a milky color until i fitered a little.Next i used a 10ml syringe with an 18 g needle to draw out 10ml of the solution. Oce i did thast i took the needle off and put a whatman 45u filter and attached the needle back on. Then i proceeded to filter the product by pushing on the syringe into a 100ml sterile and sealed vial once i got the first 10ml in there i took the filter off and attached just the needle on to it to draw another 10ml out of the solution. then once that was done i took the needle off attached the filter back on and put needle back on. Then again i proceeded to filter the contents by pushing on the syringe into the 100ml vial once i got halfway thru that period it started to get very difficult to push and liquid thru and again i just stopped coming out. Like i said before it sems to me that the powder that i received is either garbage or they might have added a cutting agent to it to increase the weight,as i know i have done the steps correctley. This is my guess now i hope you pros out there can give me an idea of what you think is going on and how to fix it i would be greatly appreciated. I was thinking about running through a cofee filter and se if that loosens it up thank john sorry for flaming you jdjack i was just pissed off for this simple thing to be over with as i have alot of money tyed up in this project of mine.

[jdjack]

Please use punctuation. This is a mess to try to discern what your asking. Giving me a headache.

[jeebise23]

dude dont waste my time u can perfectly read it

[samax64]

Originally Posted by jeebise23

dude dont waste my time u can perfectly read it

Bro he is trying to help the first mistake that I see is you put water in your pot if I read it right ..... You just wasted 50 grams of powder if that was what you said ... If that was not the case then looks like you took it off the heat to early if it was cloudy ... I didn't run your numbers but those two are enough to start with.. your numbers look wrong as well bro.... test e powder should pretty much melt in your hand if I remember right and is sort of waxy .. Plus bro if my spelling didn't suck like yours I would not have made most of that out run spell check and you might get more help

[holstein]

Now you have to capitalize the proper letters....Jesus man, where did you learn to write?

Looks like you screwed up the solution. Do you have a thermometer? Test e has a low melting point. Also, you do not need 18% BB, hell no, not with test e. Heat the mixture to 90 Celcius, stir, and you have a perfectly unsterile solution. Let it cool to whatever temp. tolerance the filter has, and filter. Get as hot as possible to the max temp of the filter so it goes through easier.

BTW, I've never heard of read of anyone cutting raws with anything. If you are not used to handling these products, then perhaps you should avoid a potential problem with your health and buy what is already made. Do not get offended, but it seems like you dont know what you are doing.

Hope it helps.

H

[samax64]

OK that looks better it seems to me like you didn't heat it up long enough... Get a candy thermometer form the grocery store for 4 buck get your beaker put the mix back in and heat it till it hit 150 and keep it there till it is clear ... how much test are you planning to make this should make you 20 bottle at 250 ?? Next if it doesn't get clear you have bad powder ???

[jdjack]

Well wanted to help but hell bro what these guys said is correct. You use water with the ba, bb, and pwdr? Its "milky". The oil or is it actually look like milk. If the oil was cloudy then you didn't heat long enough or with enough heat.

I've never heard of anyone "cutting" product like in other things in life as that would end up in a bad reputation and no more buyers.

[DragonRider]

Originally Posted by jeebise23

Hey guys this post has been revised: I am having problems with my whatman 45u getting clogged after my 2nd 10ml try.
This is how I started and finished.
First, I put 50 grams of test-e powder in a beeker. Then I added 2%=4ml of ba in, then 18%=36 ml of bb. to the powder to dissolve it.
I placed the beeker inside a pan with water in it (the pan not the beaker) and the temp. on low, and stirred it until everything was dissolved. Once that was complete, I put cottonseed oil to the mixture. I left the stove on low and kept stirring until I felt that it was enough.
Now, a lot of you guys say that it should already look clear and yellow. Well, mine was a milky colored until I filtered a little.
Next, I used a 10ml syringe with an 18g needle to draw out 10ml of the solution. Once I did that, I took the needle off and put a whatman 45u filter and attached the needle back on.
Then, I proceeded to filter the product by pushing on the syringe into a 100ml sterile and sealed vial. Once I got the first 10ml in there, I took the filter off and attached just the needle on to it to draw another 10ml out of the solution. Then once that was done, I took the needle off, attached the filter back on and put needle back on. Then again, I proceeded to filter the contents by pushing on the syringe into the 100ml vial. Once I got halfway through that period, it started to get very difficult to push the liquid through and clogged up the filter.
Like I said before, it seems to me that the powder that I received is either garbage or they might have added a cutting agent to it to increase the weight, as I know I have done the steps correctly. This is my guess.
Now I hope you pros out there can give me an idea of what you think is going on and how to fix it. It would be greatly appreciated.
I was thinking about running it through a coffee filter to see if that loosens it up.
Thank john. Sorry for flaming you jdjack. I was just pissed off for this simple thing to be over with as I have a lot of money tied up in this project of mine.

50 grams? How much were you making? 15 grams will make 50ml at 300mg/ml.

How much oil did you add to the powder? It appears as though you clogged your filter by not adding enough oil to 50 grams of powder.
50 grams of powder would have required 165ml of oil to make approximately 300mg/ml or 200ml of oil to make 250mg/ml (minus your Ba and BB of course)